What are the precautions for using the rotary evaporator?

There are many problems that need to be paid attention to during the use of the rotary evaporator. If it is used improperly, it is easy to cause damage to the rotary evaporator. Therefore, the user needs to master the precautions for use. Today we will introduce the use of rotary evaporators, I hope to help everyone.

1. The glass parts should be handled gently and gently, and should be washed, dried or dried before loading.

2. Each grinding port, sealing surface sealing ring and joints need to be coated with a layer of vacuum grease before installation.

3. The heating tank must be filled with water before it is energized. It is not allowed to dry without water.

4RE-52B must be screwed into the fuse hole (19) to avoid damage to the flask.

5. If the vacuum cannot be pumped up, check it.

(1) Each joint, whether the interface is sealed

(2) Sealing ring, whether the sealing surface is effective

(3) Is the vacuum grease between the main shaft and the seal ring coated?

(4) Whether the vacuum pump and its hose are leaking

(5) Whether the glass piece has cracks, chipping or damage

6. About the degree of vacuum

Vacuum is the most important process parameter of a rotary evaporator, and users often encounter vacuum problems. This is often related to the nature of the solvent used. Biochemical and pharmaceutical industries often use water, ethanol, acetic acid, petroleum ether, chloroform, etc. as a solvent. Generally, vacuum pumps cannot withstand strong organic solvents, and special vacuum pumps with strong corrosion resistance can be selected. (Recommended to use water circulation vacuum pump, available from the company)

The method of checking whether the instrument leaks: one by one pinch off the external vacuum tube, observe the vacuum gauge on the instrument, can keep it for five minutes without leaking. In the event of a leak, check that the seals on each seal joint and the rotating shaft are valid (see Maintenance). Conversely, the instrument is normally checked for vacuum pumps and vacuum lines.

7. About motor temperature rise

The motor of the instrument adopts three-phase, 220V special motor, E-class insulation, and the winding adopts polyester high-strength enameled wire. When the altitude is less than 1000m and the ambient temperature does not exceed 40°C, the surface temperature rise of the motor is continuously used (motor surface temperature and ambient temperature). The difference is not more than 45 ° C is normal, if the temperature rise exceeds 45 ° C to check the relevant transmission lubrication system.

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